Intergranular Corrosion Test (IGC) per ASTM A At TCR Engineering Services, several methods exist for the testing of intergranular corrosion. To conduct. Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels. ASTM A is the specification which governs five practices used to determine if the. Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the.
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Share on Tumblr Print. If you are not sure, please contact us for assistance. More suitable alternatives are offered in Table 5, below. Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice.
The ASTM A tests can determine if the proper heat treatment was performed or if the alloys are in danger of intergranular corrosion occurring aetm use. It has been used for the duplex stainless steel UNS Swhich has been used for nitric acid cooler tubes. Just remember that these tests were devised for specific groups of alloys and should not be applied to all CRAs! The chart below comes from the ASTM A standard for selection of the astn test by alloy type:. This method is preferable for chromium depletions and corrosion in intermetallic phases.
A recent publication on intergranular corrosion. Wilson Hardness Conversion Chart. Intergranular corrosion occurs as a result of precipitation of nitridescarbidesand other intermetallic phasessuch as sigma phase, that occurs along the grain boundaries. Based on your materials, application, and requirements, the other 4 methods provide specific focuses.
Contact us by Phone or Email to find aetm how we can help your industry. Asttm an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on adtm batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.
The test evaluates the resistance of extra-low-carbon steels to sensitization and intergranular attack from welding or heat treatment processes. Duplicate samples from both sides of a sheet sample are evaluated to determine if carburization results in intergranular attack. At the conclusion off the test, specimens are either visually examined or measured for weight loss and compared to an established corrosion rate for that specific material type.
The Huey test works well to analyze chromium depleted regions and intermetallic asttm, such as wstm phase, and is also used for materials in strongly oxidizing environments such as nitric acid.
ISO is specifically for duplex and all austenitic stainless steels, and recommends ageing at two different temperatures:. Plating and Coating Testing. Practice A, the oxalic acid etch test is used as a rapid technique to screen samples of certain stainless steel grades to ensure they astmm not susceptible to intergranular attack sensitization. When a test has been selected, follow the detailed directions in that standard for making up the test solution, the preparation of test samples and the finish to be used.
Make an Enquiry Notice: The test uses a visual inspection of the surface of the bent specimen to determine pass or fail.
Where a standard is included in a purchase specification, this must be followed, although it is advised that unsuitable tests, such as the Huey test for duplex and super austenitic stainless steels, are queried. ASTM A testing is a popular method of choice due to the variety of practices available and the relatively short turnaround for results. These tests do not provide a basis for predicting resistance to forms of corrosion other than intergranular, such as general corrosion, pitting, or stress-corrosion cracking.
Carbon and Sulfur Analysis. ASTM G28 lists alloys and specifies the test exposure for each.
Intergranular Corrosion Tests for CRAs
It can be seen that some alloys fall into two categories, and no guidelines are given for selecting the most appropriate. This abstract is a brief summary of the referenced standard.
Strauss test specimens are boiled in a Copper Sulfate – Sulfuric Acid mixture for 15 hours. This test is used exclusively to determine corrosion in areas high in chromium carbide formations, and is not as effective for intergranular attack caused by other means.
The inch-pound equivalents are in parentheses and may be approximate. Practice A is a rapid screening examination of the microstructure to quickly determine if the structure is certain to be free of susceptibility to rapid intergranular attack.
How do you select the right ASTM corrosion testing method for your material?
Intergranular Attack – ASTM A – Colorado-Metallurgical-Services
The bent samples are examined at low magnification, where the appearance of cracks or fissures indicate intergranular attack. Rockwell or Superficial Hardness. Where no specific test is specified, Table 5 suggests the most appropriate alongside a second choice, if the first is declined. From macroscopic imaging to Scanning Electron Microscopy, Element provides turnkey metallographic services using state-of-the-art equipment.
This practice includes boiling the sample for 24 to hours in the solution above, and measures the materials performance quantitatively. For an satm that is not listed, look for an alloy with a similar composition to a listed alloy to determine the most suitable test. The level of corrosion is determined by mass loss. This test should be avoided for most CRAs, except in the circumstances described below, in section 4. Each ASTM A Practice specification includes a list of the grades of stainless steels and the acceptable etch structures for the specific alloys.
Practice F, is a hour weight-loss based analysis that provides a quantitative measure of the materials performance, and is commonly used to analyze as-received stainless steels.